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To the several-min try (Fig. 3F), the massive diamond cereals are the main composition, since the evidenced by inset FFT image of diamond (111) diffraction areas and also the Raman range in the Si Appendix, Fig. S5, which is similar to that of the brand new 0-min test, guaranteeing the graphite provides totally transformed into diamond and formed a bulk diamond crystal compared to the original (two to four min) and you will next cycles (6 to 8 minute). These types of results definitely verify that the newest combined appearance of diamond (111) and you may graphite (002) in the sample 8-minute is actually a great transitional period of graphite in order to diamond. Phony diamond plays a vital role in the design industry, jewellery, and you may upcoming photoelectronic gizmos, but it’s an option challenge to prepare the required high-town expensive diamonds.
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- The brand new 0-s sample (Fig. 2A) displays higher rod-including diamond crystals evidenced by diffraction areas in the diamond (111) orientation regarding the inset Fourier changes (FFT) photo.
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Concurrently, an excellent flake-such diamond crystal (red photo inside Fig. 2D-2) shows that diamond starts to appear, inside the an excellent agreement to your SEM and you will Raman spectra. For the 120-s attempt, of many nanodiamond deposits naked to the edge of cauliflower-such as dust protected the brand new graphite nanorods (Fig. 2E-2). This type of performance prove the new NCD characteristics observed in the new Raman spectrum.